Invited Speaker: Andrew Minor - 4D-STEM of soft materials

17:30 – 18:10 GMT, 2 March 2022 ‐ 40 mins

Invited Speaker

This talk will highlight recent advances in direct imaging of polymer structure via 4D-STEM (nanobeam diffraction imaging).  Through the development of fast direct electron detectors, it is now possible to acquire large multidimensional diffraction data sets that can map local structural order and strain with nanometer precision, even during in situ nanomechanical testing.  The method is widely applicable and examples will be given from systems such as organic semiconductor molecular thin films, nanoparticles and even nominally amorphous samples.  This talk will describe our recent results that demonstrate the first simultaneous cryogenic 4D-STEM mapping of amorphous and crystalline structure at an interface in a semicrystalline polymer blend using a single low-dose data acquisition.  Lastly, recent developments in fast direct electron detector technology and algorithm development promise to increase the throughput, ease of use and widespread applicability of 4D-STEM.